%X A mesoporous zeolite silica alumina supported catalyst was impregnated with 3 Fe using different method of impregnation. This study focusing in finding the best impregnation method with the highest metal loaded and highly dispersion of impregnated metal. The impregnation methods carried out are wet impregnation, sono-chemical impregnation and point zero charge (PZC) impregnation. All prepared catalysts were analysed using AAS and FESEM to see the effective impregnation method. Based on the result, sono-chemical impregnation showed the highest actual Fe impregnated into the supported catalyst at 2.6 wt. and 4.0 wt. as detected by AAS and FESEM-EDX respectively. © Published under licence by IOP Publishing Ltd. %K Alumina; Aluminum oxide; Atomic absorption spectrometry; Impregnation; Silica; Zeolites, Impregnation methods; Mesoporous zeolite; Physicochemical property; Point zero charge; Preparation method; Silica-alumina; Wet impregnation, Catalyst supports %D 2018 %R 10.1088/1742-6596/1123/1/012061 %N 1 %O cited By 1; Conference of 5th International Conference on Fundamental and Applied Sciences, ICFAS 2018 ; Conference Date: 13 August 2018 Through 15 August 2018; Conference Code:142772 %J Journal of Physics: Conference Series %L scholars9590 %T Effect of preparation method on physicochemical properties of Fe/zeolite catalyst %I Institute of Physics Publishing %A A. Fakruldin %A A. Ramli %A M.I. Abdul Mutalib %V 1123