@article{scholars9431, title = {Rapid-synthesis of zeolite T via sonochemical-assisted hydrothermal growth method}, year = {2017}, doi = {10.1016/j.ultsonch.2016.05.033}, pages = {273--280}, journal = {Ultrasonics Sonochemistry}, volume = {34}, note = {cited By 36}, publisher = {Elsevier B.V.}, keywords = {Mesoporous materials; Microporous materials; Zeolites, Hydrothermal growth; Microporous and mesoporous materials; Physicochemical property; Pretreatment methods; Rapid synthesis; Sonochemical; Synthesis durations; Zeolite T, Hydrothermal synthesis, unclassified drug; zeolite; zeolite T, Article; Brunauer Emmett teller analysis; chemical procedures; chemical structure; controlled study; crystallization; field emission scanning electron microscopy; hydrogen bond; hydrothermal growth method; infrared spectroscopy; physical chemistry; priority journal; reaction analysis; sonochemical assisted method; synthesis; X ray diffraction; article; treatment duration}, url = {https://www.scopus.com/inward/record.uri?eid=2-s2.0-84971529394&doi=10.1016\%2fj.ultsonch.2016.05.033&partnerID=40&md5=aa9a5d71a7f6cfb6ea9fed438d2ab02a}, author = {Jusoh, N. and Yeong, Y. F. and Mohamad, M. and Lau, K. K. and Shariff, A. M.}, issn = {13504177}, abstract = {Sonochemical-assisted method has been identified as one of the potential pre-treatment methods which could reduce the formation duration of zeolite as well as other microporous and mesoporous materials. In the present work, zeolite T was synthesized via sonochemical-assisted pre-treatment prior to hydrothermal growth. The durations for sonochemical-assisted pre-treatment were varied from 30 min to 90 min. Meanwhile, the hydrothermal growth durations were ranged from 0.5 to 3 days. The physicochemical properties of the resulting samples were characterized using XRD, FESEM, FTIR and BET. As verified by XRD, the samples synthesized via hydrothermal growth durations of 1, 2 and 3 days and sonochemical-assisted pre-treatment durations of 60 min and 90 min demonstrated zeolite T structure. The samples which underwent sonochemical-assisted pre-treatment duration of 60 min yielded higher crystallinity with negligible change of zeolite T morphology. Overall, the lengthy synthesis duration of zeolite T has been successfully reduced from 7 days to 1 day by applying sonochemical-assisted pre-treatment of 60 min, while synthesis duration of 0.5 days via sonochemical-assisted pre-treatment of 60 min was not sufficient to produce zeolite T structure. {\^A}{\copyright} 2016 Published by Elsevier B.V.} }