eprintid: 7412 rev_number: 2 eprint_status: archive userid: 1 dir: disk0/00/00/74/12 datestamp: 2023-11-09 16:19:13 lastmod: 2023-11-09 16:19:13 status_changed: 2023-11-09 16:09:18 type: conference_item metadata_visibility: show creators_name: Ayoub, M. creators_name: Ullah, S. creators_name: Inayat, A. creators_name: Bhat, A.H. creators_name: Hailegiorgis, S.M. title: Process Optimization for Biodiesel Production from Waste Frying Oil over Montmorillonite Clay K-30 ispublished: pub keywords: Alternative fuels; Biodiesel; Catalysts; Clay; Clay minerals; Design of experiments; Driers (materials); Fossil fuel deposits; Fossil fuels; Methanol; Optimization; Palm oil; Process engineering; Transesterification, Central composite designs; Environmental concerns; Fossil fuel resources; Reaction temperature; Response surface methodology; Transesterification process; Waste frying oil; Waste frying palm oil, Well stimulation note: cited By 18; Conference of 4th International Conference on Process Engineering and Advanced Materials, ICPEAM 2016 ; Conference Date: 15 August 2016 Through 17 August 2016; Conference Code:131138 abstract: Biodiesel that mostly comes from pure renewable resources provide an alternative fuel option for future because of limited fossil fuel resources as well as environmental concerns. The transesterification of non-edible oils for biodiesel production is one of the promising process for biodiesel production to overcome this future crises of energy. The utilization of waste frying oil into biodiesel have great worth for economization of biodiesel cost as well as the conversion of waste into value added product with environmental protection. The purpose of the present work is to optimize the process of biodiesel production over a heterogeneous clay based catalyst. Particularly, the transesterification of waste frying palm oil with methanol was studied in the presence of montmorillonite clay K-30 as solid base catalyst that have both of acid and basic nature. The observed date was then optimized with the help of Design of Experiments software. The Response Surface Methodology (RSM) based on four-variable central composite design (CCD) with α (alpha) = 2 was used for this purpose. The transesterification process variables were reaction temperature, x1 (40-140oC), reaction period, x2 (60-300 min), methanol/oil ratio, x3 (6:1- 18:1 mol/ mol) and amount of catalyst, x4 (1-5 wt). The results showed that waste frying oil is a good feedstock for biodiesel production and high yield of 78.4 was obtained during optimization of this biodiesel process that was noted after 180 min at temperature 90°C, with a 12:1molar ratio of methanol to waste frying oil and using 3wt of montmorillonite clay K-30 catalyst. © 2016 The Authors. date: 2016 publisher: Elsevier Ltd official_url: https://www.scopus.com/inward/record.uri?eid=2-s2.0-85014015256&doi=10.1016%2fj.proeng.2016.06.606&partnerID=40&md5=a5e00088102dc858c903c412819b27f6 id_number: 10.1016/j.proeng.2016.06.606 full_text_status: none publication: Procedia Engineering volume: 148 pagerange: 742-749 refereed: TRUE issn: 18777058 citation: Ayoub, M. and Ullah, S. and Inayat, A. and Bhat, A.H. and Hailegiorgis, S.M. (2016) Process Optimization for Biodiesel Production from Waste Frying Oil over Montmorillonite Clay K-30. In: UNSPECIFIED.