eprintid: 6635 rev_number: 2 eprint_status: archive userid: 1 dir: disk0/00/00/66/35 datestamp: 2023-11-09 16:18:25 lastmod: 2023-11-09 16:18:25 status_changed: 2023-11-09 16:07:15 type: conference_item metadata_visibility: show creators_name: Sulong, T.S.T. creators_name: Zabidi, N.A.M. creators_name: Shaharun, M.S. title: Pretreatment of carbon nanotubes: Effects on its properties and catalytic performances ispublished: pub note: cited By 0; Conference of 4th International Conference on Fundamental and Applied Sciences, ICFAS 2016 ; Conference Date: 15 August 2016 Through 17 August 2016; Conference Code:125141 abstract: The effects of pretreatment via acid and thermal treatment on the properties of multi-walled carbon nanotubes (MWCNTs) are studied using FTIR, TGA, Raman spectroscopy and TEM. Meanwhile, catalytic performances of Cu/ZnO catalysts supported on raw and treated CNTs are evaluated by CO2 hydrogenation into methanol using a fixed-bed microactivity reactor. Pretreatment of CNTs have removed caps, created defects on CNTs wall and also introduced some functional groups as confirmed by FTIR, TGA, Raman spectroscopy and TEM. However, deposition of metals into the support via incipient wetness impregnation method results in agglomeration of metal particles outside CNTs. Methanol synthesis studies (523 K, 22.5 bar) were performed and activity study revealed that catalysts supported on treated CNTs achieved CO2 conversion of 19 . © 2016 Author(s). date: 2016 publisher: American Institute of Physics Inc. official_url: https://www.scopus.com/inward/record.uri?eid=2-s2.0-85005982542&doi=10.1063%2f1.4968077&partnerID=40&md5=a555f7136e61f999d039c5d9541195fd id_number: 10.1063/1.4968077 full_text_status: none publication: AIP Conference Proceedings volume: 1787 refereed: TRUE isbn: 9780735414518 issn: 0094243X citation: Sulong, T.S.T. and Zabidi, N.A.M. and Shaharun, M.S. (2016) Pretreatment of carbon nanotubes: Effects on its properties and catalytic performances. In: UNSPECIFIED.