relation: https://khub.utp.edu.my/scholars/6374/ title: Surface Hardening of M2 High Speed Steel Using 50 Hz Pulsed DC Source with Nitrogen as a Base Gas creator: Naz, M.Y. creator: Shukrullah, S. creator: Javaid, M.A. creator: Ghaffar, A. creator: Rehman, N.U. description: Plasma processing provides a useful tool for modifying the metallic and non-metallic surfaces. Plasma ion nitriding of M2 high-speed steel was carried out by using a low pressure plasma chamber and a 50 Hz pulsed DC source. By keeping the nitrogen-hydrogen (60:40) mixture pressure constant at 3 mbar and varying the plasma treatment time from 1 to 4 h, the nitriding was done in the abnormal glow region at 600°C substrate temperature. The resultant changes in surface properties of the plasma treated samples were investigated by using X-ray diffraction, scanning electron microscopy, and Vickers's microhardness testing. These investigations confirmed the formation of a compound layer on plasma exposed surface. The layer thickness was initially increased with nitriding time and then started to decrease after 2 h treatment. In X-ray diffraction data, a down-shift in the original diffraction peaks was noticed which confirms the nitrogen diffusion and formation of compound layer on the exposed surface. A significant improvement in surface hardness of tool steel was also seen especially after 2 h of plasma treatment. Copyright © Taylor & Francis Group, LLC. publisher: Taylor and Francis Inc. date: 2015 type: Article type: PeerReviewed identifier: Naz, M.Y. and Shukrullah, S. and Javaid, M.A. and Ghaffar, A. and Rehman, N.U. (2015) Surface Hardening of M2 High Speed Steel Using 50 Hz Pulsed DC Source with Nitrogen as a Base Gas. Synthesis and Reactivity in Inorganic, Metal-Organic and Nano-Metal Chemistry, 45 (7). pp. 1057-1062. ISSN 15533174 relation: https://www.scopus.com/inward/record.uri?eid=2-s2.0-84924402479&doi=10.1080%2f15533174.2013.862653&partnerID=40&md5=9d8696e6e97b255903bcd222e5b2331b relation: 10.1080/15533174.2013.862653 identifier: 10.1080/15533174.2013.862653