eprintid: 5861 rev_number: 2 eprint_status: archive userid: 1 dir: disk0/00/00/58/61 datestamp: 2023-11-09 16:17:36 lastmod: 2023-11-09 16:17:36 status_changed: 2023-11-09 16:04:04 type: conference_item metadata_visibility: show creators_name: Adil, M. creators_name: Zaid, H.M. creators_name: Chuan, L.K. creators_name: Alta'Ee, A.F. creators_name: Latiff, N.R.A. title: Microscopic evolution of dielectric nanoparticles at different calcination temperatures synthesized via sol-gel auto-combustion ispublished: pub note: cited By 13; Conference of 23rd Scientific Conference of Microscopy Society Malaysia, SCMSM 2014 ; Conference Date: 10 December 2014 Through 12 December 2014; Conference Code:113582 abstract: Dielectric nano powder synthesis is carried by a simple and fast sol-gel auto-combustion method. The transformation of crystalline phases of as-synthesized nano powders is investigated through the detailed transmission electron microscopy (TEM), revealed the crystallographic alterations and morphological information even at lattice scale. From specific area electron diffraction (SAED) pattern, has specified the d-spacing and corresponding planes supported by the observed lattice fringes. The morphological characterization of nanoparticles is performed through field-emission scanning electron microscopy (FESEM), exhibiting the increment in particle size due to agglomeration with the increase in annealing temperature. Furthermore, EDX pattern has been used to verify the formation of nanoparticles by revealing the presence of required elements. © 2015 AIP Publishing LLC. date: 2015 publisher: American Institute of Physics Inc. official_url: https://www.scopus.com/inward/record.uri?eid=2-s2.0-85043613188&doi=10.1063%2f1.4919154&partnerID=40&md5=135a007554e7a1eb0fa5b22f8763d5f2 id_number: 10.1063/1.4919154 full_text_status: none publication: AIP Conference Proceedings volume: 1669 refereed: TRUE isbn: 9780735413160 issn: 0094243X citation: Adil, M. and Zaid, H.M. and Chuan, L.K. and Alta'Ee, A.F. and Latiff, N.R.A. (2015) Microscopic evolution of dielectric nanoparticles at different calcination temperatures synthesized via sol-gel auto-combustion. In: UNSPECIFIED.