eprintid: 5696
rev_number: 2
eprint_status: archive
userid: 1
dir: disk0/00/00/56/96
datestamp: 2023-11-09 16:17:26
lastmod: 2023-11-09 16:17:26
status_changed: 2023-11-09 16:03:37
type: article
metadata_visibility: show
creators_name: Lieu, T.
creators_name: Yusup, S.
creators_name: Moniruzzaman, M.
title: Parametric study of esterification of free fatty acids derived from Ceiba Pentandra seed oil using microwaveassisted technique via response surface methodology
ispublished: pub
keywords: Alternative fuels; Biodiesel; Catalysts; Esters; Feedstocks; Methanol; Oils and fats; Organic solvents; Vegetable oils, Acid esterification; Biodiesel production; Edible vegetable oil; Esterification of free fatty acids; High free fatty acids; Microwave-assisted technique; Potential feedstock; Response surface methodology, Fatty acids
note: cited By 1
abstract: Biodiesel is an alternative fuel to conventional petroleum diesel. Due to economic and social concerns, the use of edible vegetable oils and animal fats should be replaced by non-edible plant oils for biodiesel production. In this regard, the oil from tropical plant Ceiba Pentandra is an attractive potential feedstock. However, like other non-edible feedstocks, C. Pentandra seed oil contains high free fatty acids (FFA) which negatively affect the process of biodiesel production. In the present work, acid esterification process was applied as a pre-treatment to reduce FFA content. By using microwave-assisted technique, the optimum conditions for diminishing the FFA content in the seed oil to 0.388  were found to be 2.0 wt H2SO4 catalyst, 10:1 methanol to oil molar ratio at 60 °C within 12 minutes of reaction time. In addition, an investigation on the effect of different acid catalysts such as hydrochloric acid and phosphoric acid as well as different solvents such as ethanol, 1-propanol and 2-propanol to obtain the best result based on optimum conditions was carried out. Sulfuric acid and methanol were found to be the best option for pretreatment of Ceiba Pentandra feedstock. Copyright © 2015, AIDIC Servizi S.r.l.,.
date: 2015
publisher: Italian Association of Chemical Engineering - AIDIC
official_url: https://www.scopus.com/inward/record.uri?eid=2-s2.0-84946137892&doi=10.3303%2fCET1545156&partnerID=40&md5=cd00939b47a9c42b765d3a32009743be
id_number: 10.3303/CET1545156
full_text_status: none
publication: Chemical Engineering Transactions
volume: 45
pagerange: 931-936
refereed: TRUE
isbn: 9788895608365
issn: 22839216
citation:   Lieu, T. and Yusup, S. and Moniruzzaman, M.  (2015) Parametric study of esterification of free fatty acids derived from Ceiba Pentandra seed oil using microwaveassisted technique via response surface methodology.  Chemical Engineering Transactions, 45.  pp. 931-936.  ISSN 22839216