eprintid: 5154
rev_number: 2
eprint_status: archive
userid: 1
dir: disk0/00/00/51/54
datestamp: 2023-11-09 16:16:52
lastmod: 2023-11-09 16:16:52
status_changed: 2023-11-09 16:00:45
type: article
metadata_visibility: show
creators_name: Lee, S.-P.
creators_name: Ramli, A.
creators_name: Kutty, M.G.
creators_name: Hamid, S.B.A.
title: Incorporation of Pd nanoparticles on rod and necklace-like SBA-15 supports materials
ispublished: pub
keywords: Inductively coupled plasma mass spectrometry; Mass spectrometers; Nanoparticles; Process engineering; Scanning electron microscopy; Thermogravimetric analysis; Transmission electron microscopy, Adsorption desorption; Inductive coupled plasma; Mesoporous SBA-15; Necklace-like; PD nano particle; Rod-like; Sba-15 supports; Thermal spectroscopy, Ion exchange
note: cited By 0; Conference of International Conference on Process Engineering and Advanced Materials, ICPEAM 2012 ; Conference Date: 12 June 2012 Through 14 June 2012; Conference Code:106208
abstract: Ion-exchange of palladium (Pd) precursor for two different types of well-ordered SBA- 15 morphologies, necklace-like and rod-like, was studied. Approximately 3.8 wt Pd was successfully incorporated into SBA-15 at pH 10.3. Formation of SBA-15 and Pd/SBA-15 were characterized by Scanning Electron Microscope (SEM), Transmission Electron Microscope (TEM), Thermogravimetry with Simultaneous Difference Thermal Spectroscopy coupled with mass spectrometer (TG/SDTA-MS), Thermogravimetry in combination with Simultaneous Difference Thermal Spectroscopy (TG-SDTA), Inductive Coupled Plasma Mass Spectrometer (ICP-MS) and N2 adsorption-desorption. Reduction of surface area and pore volume of support for Pd/SBA-15 samples may indicate the encapsulation of PdO particles within mesoporous channels of SBA-15. © (2014) Trans Tech Publications, Switzerland.
date: 2014
publisher: Trans Tech Publications Ltd
official_url: https://www.scopus.com/inward/record.uri?eid=2-s2.0-84904068481&doi=10.4028%2fwww.scientific.net%2fAMR.917.10&partnerID=40&md5=e834aa370140ff72febcbf4dd3fbe68f
id_number: 10.4028/www.scientific.net/AMR.917.10
full_text_status: none
publication: Advanced Materials Research
volume: 917
place_of_pub: Kuala Lumpur
pagerange: 10-17
refereed: TRUE
isbn: 9783038350521
issn: 10226680
citation:   Lee, S.-P. and Ramli, A. and Kutty, M.G. and Hamid, S.B.A.  (2014) Incorporation of Pd nanoparticles on rod and necklace-like SBA-15 supports materials.  Advanced Materials Research, 917.  pp. 10-17.  ISSN 10226680