TY  - JOUR
KW  - Inductively coupled plasma mass spectrometry; Mass spectrometers; Nanoparticles; Process engineering; Scanning electron microscopy; Thermogravimetric analysis; Transmission electron microscopy
KW  -  Adsorption desorption; Inductive coupled plasma; Mesoporous SBA-15; Necklace-like; PD nano particle; Rod-like; Sba-15 supports; Thermal spectroscopy
KW  -  Ion exchange
ID  - scholars5154
N2  - Ion-exchange of palladium (Pd) precursor for two different types of well-ordered SBA- 15 morphologies, necklace-like and rod-like, was studied. Approximately 3.8 wt Pd was successfully incorporated into SBA-15 at pH 10.3. Formation of SBA-15 and Pd/SBA-15 were characterized by Scanning Electron Microscope (SEM), Transmission Electron Microscope (TEM), Thermogravimetry with Simultaneous Difference Thermal Spectroscopy coupled with mass spectrometer (TG/SDTA-MS), Thermogravimetry in combination with Simultaneous Difference Thermal Spectroscopy (TG-SDTA), Inductive Coupled Plasma Mass Spectrometer (ICP-MS) and N2 adsorption-desorption. Reduction of surface area and pore volume of support for Pd/SBA-15 samples may indicate the encapsulation of PdO particles within mesoporous channels of SBA-15. © (2014) Trans Tech Publications, Switzerland.
CY  - Kuala Lumpur
VL  - 917
UR  - https://www.scopus.com/inward/record.uri?eid=2-s2.0-84904068481&doi=10.4028%2fwww.scientific.net%2fAMR.917.10&partnerID=40&md5=e834aa370140ff72febcbf4dd3fbe68f
JF  - Advanced Materials Research
A1  - Lee, S.-P.
A1  - Ramli, A.
A1  - Kutty, M.G.
A1  - Hamid, S.B.A.
Y1  - 2014///
TI  - Incorporation of Pd nanoparticles on rod and necklace-like SBA-15 supports materials
SP  - 10
N1  - cited By 0; Conference of International Conference on Process Engineering and Advanced Materials, ICPEAM 2012 ; Conference Date: 12 June 2012 Through 14 June 2012; Conference Code:106208
AV  - none
EP  - 17
SN  - 10226680
PB  - Trans Tech Publications Ltd
ER  -