@article{scholars5154, year = {2014}, publisher = {Trans Tech Publications Ltd}, journal = {Advanced Materials Research}, pages = {10--17}, note = {cited By 0; Conference of International Conference on Process Engineering and Advanced Materials, ICPEAM 2012 ; Conference Date: 12 June 2012 Through 14 June 2012; Conference Code:106208}, volume = {917}, doi = {10.4028/www.scientific.net/AMR.917.10}, title = {Incorporation of Pd nanoparticles on rod and necklace-like SBA-15 supports materials}, address = {Kuala Lumpur}, abstract = {Ion-exchange of palladium (Pd) precursor for two different types of well-ordered SBA- 15 morphologies, necklace-like and rod-like, was studied. Approximately 3.8 wt Pd was successfully incorporated into SBA-15 at pH 10.3. Formation of SBA-15 and Pd/SBA-15 were characterized by Scanning Electron Microscope (SEM), Transmission Electron Microscope (TEM), Thermogravimetry with Simultaneous Difference Thermal Spectroscopy coupled with mass spectrometer (TG/SDTA-MS), Thermogravimetry in combination with Simultaneous Difference Thermal Spectroscopy (TG-SDTA), Inductive Coupled Plasma Mass Spectrometer (ICP-MS) and N2 adsorption-desorption. Reduction of surface area and pore volume of support for Pd/SBA-15 samples may indicate the encapsulation of PdO particles within mesoporous channels of SBA-15. {\^A}{\copyright} (2014) Trans Tech Publications, Switzerland.}, url = {https://www.scopus.com/inward/record.uri?eid=2-s2.0-84904068481&doi=10.4028\%2fwww.scientific.net\%2fAMR.917.10&partnerID=40&md5=e834aa370140ff72febcbf4dd3fbe68f}, keywords = {Inductively coupled plasma mass spectrometry; Mass spectrometers; Nanoparticles; Process engineering; Scanning electron microscopy; Thermogravimetric analysis; Transmission electron microscopy, Adsorption desorption; Inductive coupled plasma; Mesoporous SBA-15; Necklace-like; PD nano particle; Rod-like; Sba-15 supports; Thermal spectroscopy, Ion exchange}, isbn = {9783038350521}, author = {Lee, S.-P. and Ramli, A. and Kutty, M. G. and Hamid, S. B. A.}, issn = {10226680} }