eprintid: 4762 rev_number: 2 eprint_status: archive userid: 1 dir: disk0/00/00/47/62 datestamp: 2023-11-09 16:16:28 lastmod: 2023-11-09 16:16:28 status_changed: 2023-11-09 15:59:23 type: article metadata_visibility: show creators_name: Ellateif, T.M.A. creators_name: Mitra, S. creators_name: Murugesan, T. creators_name: Azizi, K. title: Preparation and characterization of hydrophobic silica zirconium nanoparticles ispublished: pub keywords: Characterization; Hydrophobicity; Nanoparticles; Sol-gel process; Sol-gels; Synthesis (chemical); Zirconium, BET analysis; Particle distributions; Pure silica; Silica nanoparticles; Silica sols; Surface area; Synthesized silica; Weight gain, Silica note: cited By 0; Conference of 3rd International Conference on Process Engineering and Advanced Materials, ICPEAM 2014 ; Conference Date: 3 June 2014 Through 5 June 2014; Conference Code:114811 abstract: Hydrophobic silica nanoparticles were synthesized by silica sols modified with different percentage of zirconium sol using liquid modification. The hydrophobicity test demonstrated that silica zirconium nanoparticles are more hydrophobic as they showed 1 to 5 weight gain compared to 8 for pure silica nanoparticles. The synthesized silica nanoparticles were characterized using different techniques to investigate the effect of zirconium modification on silica nanoparticles characteristics. Structure and composition of unmodified silica nanoparticles and modified one were studied using FTIR; the results showed that the zirconium oxide was anchored to the surface of silica nanoparticles. TEM and BET analysis showed that the percentage of zirconium added to silica had distinct effect on the particle distribution and surface area of silica nanoparticles. © 2014 Trans Tech Publications, Switzerland. date: 2014 publisher: Trans Tech Publications Ltd official_url: https://www.scopus.com/inward/record.uri?eid=2-s2.0-84914133361&doi=10.4028%2fwww.scientific.net%2fAMM.625.503&partnerID=40&md5=5f9ff54411335e6aab0070e29f72a1a2 id_number: 10.4028/www.scientific.net/AMM.625.503 full_text_status: none publication: Applied Mechanics and Materials volume: 625 pagerange: 503-508 refereed: TRUE isbn: 9783038351818 issn: 16609336 citation: Ellateif, T.M.A. and Mitra, S. and Murugesan, T. and Azizi, K. (2014) Preparation and characterization of hydrophobic silica zirconium nanoparticles. Applied Mechanics and Materials, 625. pp. 503-508. ISSN 16609336