%0 Journal Article
%@ 09226168
%A Mohd Ibrahim, S.
%A Masrom, A.K.
%A Mazinani, B.
%A Radiman, S.
%A Md Jamil, F.
%A Beitollahi, A.
%A Negishi, N.
%A Yahya, N.
%D 2013
%F scholars:3711
%J Research on Chemical Intermediates
%K Field emission scanning electron microscopy; High photocatalytic activities; Mesoporous; Non-ionic triblock copolymers; Photocatalytic activities; Photodegradation of methylene blue; TiO; UV visible spectroscopy, Aromatic compounds; Block copolymers; Calcination; Differential thermal analysis; Field emission microscopes; Photocatalysis; Photocatalysts; Sol-gel process; Surface active agents; Thermogravimetric analysis; Titanium dioxide; Transmission electron microscopy; Ultraviolet visible spectroscopy, Mesoporous materials
%N 3
%P 1003-1014
%R 10.1007/s11164-012-0611-0
%T Mesoporous titania photocatalyst: Effect of relative humidity and aging on the preparation of mesoporous titania and on its photocatalytic activity performance
%U https://khub.utp.edu.my/scholars/3711/
%V 39
%X Mesoporous TiO2 has been synthesized by the sol-gel method, using a nonionic triblock copolymer P123 as surfactant template under acidic conditions. The as-prepared samples were characterized by thermogravimetry- differential thermal analysis (TG-DTA), nitrogen absorption-desorption (BET), field emission scanning electron microscopy, and transmission electron microscopy. The photocatalytic activity of the mesoporous TiO2 was evaluated by degradation of methylene blue under high-intensity UV light irradiation; the amount of methylene blue was measured by UV-visible spectroscopy. TG-DTA analysis revealed that the surfactant had been removed partly in as-synthesized samples. BET analysis proved that all the samples retained mesoporosity with a narrow pore-size distribution (4.5-6.3 nm) and high surface area (103-200 m2/g). All calcined mesoporous TiO2 had high photocatalytic activity in the photodegradation of methylene blue. © 2012 Springer Science+Business Media B.V.
%Z cited By 8