relation: https://khub.utp.edu.my/scholars/3711/ title: Mesoporous titania photocatalyst: Effect of relative humidity and aging on the preparation of mesoporous titania and on its photocatalytic activity performance creator: Mohd Ibrahim, S. creator: Masrom, A.K. creator: Mazinani, B. creator: Radiman, S. creator: Md Jamil, F. creator: Beitollahi, A. creator: Negishi, N. creator: Yahya, N. description: Mesoporous TiO2 has been synthesized by the sol-gel method, using a nonionic triblock copolymer P123 as surfactant template under acidic conditions. The as-prepared samples were characterized by thermogravimetry- differential thermal analysis (TG-DTA), nitrogen absorption-desorption (BET), field emission scanning electron microscopy, and transmission electron microscopy. The photocatalytic activity of the mesoporous TiO2 was evaluated by degradation of methylene blue under high-intensity UV light irradiation; the amount of methylene blue was measured by UV-visible spectroscopy. TG-DTA analysis revealed that the surfactant had been removed partly in as-synthesized samples. BET analysis proved that all the samples retained mesoporosity with a narrow pore-size distribution (4.5-6.3 nm) and high surface area (103-200 m2/g). All calcined mesoporous TiO2 had high photocatalytic activity in the photodegradation of methylene blue. © 2012 Springer Science+Business Media B.V. date: 2013 type: Article type: PeerReviewed identifier: Mohd Ibrahim, S. and Masrom, A.K. and Mazinani, B. and Radiman, S. and Md Jamil, F. and Beitollahi, A. and Negishi, N. and Yahya, N. (2013) Mesoporous titania photocatalyst: Effect of relative humidity and aging on the preparation of mesoporous titania and on its photocatalytic activity performance. Research on Chemical Intermediates, 39 (3). pp. 1003-1014. ISSN 09226168 relation: https://www.scopus.com/inward/record.uri?eid=2-s2.0-84876491828&doi=10.1007%2fs11164-012-0611-0&partnerID=40&md5=43a2dfc2a84d8f0ac58578cf77b3320a relation: 10.1007/s11164-012-0611-0 identifier: 10.1007/s11164-012-0611-0