eprintid: 17911
rev_number: 2
eprint_status: archive
userid: 1
dir: disk0/00/01/79/11
datestamp: 2023-12-19 03:24:13
lastmod: 2023-12-19 03:24:13
status_changed: 2023-12-19 03:08:54
type: article
metadata_visibility: show
creators_name: Rozaini, M.N.H.
creators_name: Saad, B.
creators_name: Yahaya, N.
creators_name: Lim, J.W.
creators_name: Mohd Aris, M.N.
creators_name: Ramachandran, M.R.
title: Determination of Three Endocrine Disruptors in Water Samples by Ultrasound-Assisted Salt-Induced Liquid-Liquid Microextraction (UA-SI-LLME) and High-Performance Liquid Chromatography�Diode Array Detection (HPLC-DAD)
ispublished: pub
note: cited By 0
abstract: Endocrine-disrupting compounds are routinely detected in environmental water. In this study, a simple and rapid sample preparation method based on ultrasound-assisted salt-induced liquid-liquid microextraction (UA-SI-LLME) followed by high performance liquid chromatography�diode array detection (HPLC-DAD) was developed for the determination of triclosan, triclocarban and methyl-triclosan in water. Parameters that affect the extraction efficiency�such as type and mass of salt, type and volume of extraction solvent, extraction time, sample pH and sample volume�were studied. Under the optimized conditions, the method demonstrated linearity from 0.18 to 1000 µg L�1 with coefficients of determination R2 � 0.9899, limits of detection from 0.05 to 0.2 µg L�1, and good recoveries (> 70) with relative standard deviations < 10. The method was applied for the determination of triclosan, triclocarban, and methyl-triclosan in swimming pool, lake, and wastewater. The greenness of the method was quantified using the Analytical Eco-Scale Index. © 2022 Taylor & Francis Group, LLC.
date: 2022
publisher: Taylor and Francis Ltd.
official_url: https://www.scopus.com/inward/record.uri?eid=2-s2.0-85106048229&doi=10.1080%2f00032719.2021.1919691&partnerID=40&md5=99bca6089af6dce8d4b978af059f1588
id_number: 10.1080/00032719.2021.1919691
full_text_status: none
publication: Analytical Letters
volume: 55
number: 1
pagerange: 132-145
refereed: TRUE
issn: 00032719
citation:   Rozaini, M.N.H. and Saad, B. and Yahaya, N. and Lim, J.W. and Mohd Aris, M.N. and Ramachandran, M.R.  (2022) Determination of Three Endocrine Disruptors in Water Samples by Ultrasound-Assisted Salt-Induced Liquid-Liquid Microextraction (UA-SI-LLME) and High-Performance Liquid Chromatography�Diode Array Detection (HPLC-DAD).  Analytical Letters, 55 (1).  pp. 132-145.  ISSN 00032719