TY  - JOUR
IS  - 1
SN  - 00032719
VL  - 55
N1  - cited By 0
TI  - Determination of Three Endocrine Disruptors in Water Samples by Ultrasound-Assisted Salt-Induced Liquid-Liquid Microextraction (UA-SI-LLME) and High-Performance Liquid Chromatographyâ??Diode Array Detection (HPLC-DAD)
AV  - none
UR  - https://www.scopus.com/inward/record.uri?eid=2-s2.0-85106048229&doi=10.1080%2f00032719.2021.1919691&partnerID=40&md5=99bca6089af6dce8d4b978af059f1588
EP  - 145
PB  - Taylor and Francis Ltd.
SP  - 132
ID  - scholars17911
Y1  - 2022///
N2  - Endocrine-disrupting compounds are routinely detected in environmental water. In this study, a simple and rapid sample preparation method based on ultrasound-assisted salt-induced liquid-liquid microextraction (UA-SI-LLME) followed by high performance liquid chromatographyâ??diode array detection (HPLC-DAD) was developed for the determination of triclosan, triclocarban and methyl-triclosan in water. Parameters that affect the extraction efficiencyâ??such as type and mass of salt, type and volume of extraction solvent, extraction time, sample pH and sample volumeâ??were studied. Under the optimized conditions, the method demonstrated linearity from 0.18 to 1000 µg Lâ??1 with coefficients of determination R2 â?¥ 0.9899, limits of detection from 0.05 to 0.2 µg Lâ??1, and good recoveries (> 70) with relative standard deviations < 10. The method was applied for the determination of triclosan, triclocarban, and methyl-triclosan in swimming pool, lake, and wastewater. The greenness of the method was quantified using the Analytical Eco-Scale Index. © 2022 Taylor & Francis Group, LLC.
A1  - Rozaini, M.N.H.
A1  - Saad, B.
A1  - Yahaya, N.
A1  - Lim, J.W.
A1  - Mohd Aris, M.N.
A1  - Ramachandran, M.R.
JF  - Analytical Letters
ER  -