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<https://khub.utp.edu.my/scholars/id/eprint/17911> <http://purl.org/dc/terms/title> "Determination of Three Endocrine Disruptors in Water Samples by Ultrasound-Assisted Salt-Induced Liquid-Liquid Microextraction (UA-SI-LLME) and High-Performance Liquid Chromatographyâ��Diode Array Detection (HPLC-DAD)"^^<http://www.w3.org/2001/XMLSchema#string> .
<https://khub.utp.edu.my/scholars/id/eprint/17911> <http://purl.org/ontology/bibo/abstract> "Endocrine-disrupting compounds are routinely detected in environmental water. In this study, a simple and rapid sample preparation method based on ultrasound-assisted salt-induced liquid-liquid microextraction (UA-SI-LLME) followed by high performance liquid chromatographyâ��diode array detection (HPLC-DAD) was developed for the determination of triclosan, triclocarban and methyl-triclosan in water. Parameters that affect the extraction efficiencyâ��such as type and mass of salt, type and volume of extraction solvent, extraction time, sample pH and sample volumeâ��were studied. Under the optimized conditions, the method demonstrated linearity from 0.18 to 1000 Âµg Lâ��1 with coefficients of determination R2 â�¥ 0.9899, limits of detection from 0.05 to 0.2 Âµg Lâ��1, and good recoveries (&gt; 70) with relative standard deviations &lt; 10. The method was applied for the determination of triclosan, triclocarban, and methyl-triclosan in swimming pool, lake, and wastewater. The greenness of the method was quantified using the Analytical Eco-Scale Index. Â© 2022 Taylor & Francis Group, LLC."^^<http://www.w3.org/2001/XMLSchema#string> .
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