relation: https://khub.utp.edu.my/scholars/17911/
title: Determination of Three Endocrine Disruptors in Water Samples by Ultrasound-Assisted Salt-Induced Liquid-Liquid Microextraction (UA-SI-LLME) and High-Performance Liquid Chromatography�Diode Array Detection (HPLC-DAD)
creator: Rozaini, M.N.H.
creator: Saad, B.
creator: Yahaya, N.
creator: Lim, J.W.
creator: Mohd Aris, M.N.
creator: Ramachandran, M.R.
description: Endocrine-disrupting compounds are routinely detected in environmental water. In this study, a simple and rapid sample preparation method based on ultrasound-assisted salt-induced liquid-liquid microextraction (UA-SI-LLME) followed by high performance liquid chromatography�diode array detection (HPLC-DAD) was developed for the determination of triclosan, triclocarban and methyl-triclosan in water. Parameters that affect the extraction efficiency�such as type and mass of salt, type and volume of extraction solvent, extraction time, sample pH and sample volume�were studied. Under the optimized conditions, the method demonstrated linearity from 0.18 to 1000 µg L�1 with coefficients of determination R2 � 0.9899, limits of detection from 0.05 to 0.2 µg L�1, and good recoveries (> 70) with relative standard deviations < 10. The method was applied for the determination of triclosan, triclocarban, and methyl-triclosan in swimming pool, lake, and wastewater. The greenness of the method was quantified using the Analytical Eco-Scale Index. © 2022 Taylor & Francis Group, LLC.
publisher: Taylor and Francis Ltd.
date: 2022
type: Article
type: PeerReviewed
identifier:   Rozaini, M.N.H. and Saad, B. and Yahaya, N. and Lim, J.W. and Mohd Aris, M.N. and Ramachandran, M.R.  (2022) Determination of Three Endocrine Disruptors in Water Samples by Ultrasound-Assisted Salt-Induced Liquid-Liquid Microextraction (UA-SI-LLME) and High-Performance Liquid Chromatography�Diode Array Detection (HPLC-DAD).  Analytical Letters, 55 (1).  pp. 132-145.  ISSN 00032719     
relation: https://www.scopus.com/inward/record.uri?eid=2-s2.0-85106048229&doi=10.1080%2f00032719.2021.1919691&partnerID=40&md5=99bca6089af6dce8d4b978af059f1588
relation: 10.1080/00032719.2021.1919691
identifier: 10.1080/00032719.2021.1919691