%K Addition of Al; Atmospheric carbon dioxide concentration; Carbon dioxide separation; Crystal size; dolomite; Fossil fuel fired power plants; Molar ratio; Phase identification; solvothermolysis; Synthetic gas mixture; Thermal decompositions; Weight loss; X-ray diffraction techniques, Adsorption; Atmospheric chemistry; Ethanol; Industrial emissions; Industrial plants; Organic solvents; Polyethylene glycols; Pyrolysis; Rhodium; Sustainable development; Thermogravimetric analysis; X ray diffraction, Carbon dioxide %X Huge emissions of carbon dioxide from fossil fuel fired power plants and industrial plants over the last century have resulted in an increase of the atmospheric carbon dioxide concentration, resulting in so-called green house. Thus development of CO 2 adsorbent seems to be crucial nowadays. In this work solvothermolysis processes was performed on dolomite with and without addition of Al(OH) 2 in molar ratio of 1:1, 1:2 and 1:3 of Al(OH) 2 to dolomite using three differences solvent which are water, ethanol and polyethylene glycol. The phase identification of solvothermolysed dolomite was performed using X-ray diffraction technique (XRD) and it was found that the samples possessed the main peaks of the raw dolomite thus conformed that they existed in Hexagonal (Rh) system. t-e-dolomite and 1:2 t-e-AL:d shows improvement in amount of CO 2 adsorbed compared to raw dolomite, the lowest average crystal size and decomposed at lowest temperature with highest weight loss in thermogravimetric analysis (TGA). © 2011 IEEE. %J 2011 National Postgraduate Conference - Energy and Sustainability: Exploring the Innovative Minds, NPC 2011 %L scholars1723 %O cited By 0; Conference of 3rd National Postgraduate Conference - Energy and Sustainability: Exploring the Innovative Minds, NPC 2011 ; Conference Date: 19 September 2011 Through 20 September 2011; Conference Code:88531 %R 10.1109/NatPC.2011.6136277 %D 2011 %A N.A. Endot %A Y. Lwin %T Characterization of novel solvothermolysed dolomite for carbon dioxide separation from synthetic gas mixture %C Perak