%X Desiccated coconut waste (DCW) is an agricultural waste that originates from the coconut milk processing industry. In this study, it was utilized for the removal of copper (Cu(II)) and nickel (Ni(II)) via adsorption process. The physicochemical characterization of the DCW adsorbent shows that the adsorbent have a surface area of 6.63 m2/g, have high elemental carbon content and existences of important functional groups on its surface. The adsorptive capability of DCW adsorbent in removing the heavy metal were conducted in batch studies. DCW adsorbent performed highest Ni(II) and Cu(II) adsorption capacity at pH 6, where equilibrium is achieved at 450 minutes. The kinetic analysis showed the adsorption agreed with pseudo-second order kinetic model, indicating the Cu(II) and Ni(II) adsorption were a chemical adsorption, limited by the film diffusion. The DCW adsorbent still retained its effective adsorption capacity after 2 adsorption-desorption cycles, which is one of the excellent criteria of a good adsorbent for an adsorption process. © 2021 Korean Society of Environmental Engineers. %K Agricultural wastes; Chemical analysis; Copper compounds; Cost effectiveness; Heavy metals; Nickel compounds, Adsorption capacities; Adsorption process; Coconut milk; Coconut wastes; Copper cu; Cost effective; Milk processing; Physico-chemical characterization; Processing industry; Regeneration, Adsorption %R 10.4491/eer.2020.250 %N 4 %D 2021 %L scholars14663 %J Environmental Engineering Research %O cited By 9 %V 26 %I Korean Society of Environmental Engineers %A A.R.A. Rahim %A Iswarya %A K. Johari %A N. Shehzad %A N. Saman %A H. Mat %T Conversion of coconut waste into cost effective adsorbent for Cu(II) and Ni(II) removal from aqueous solutions