eprintid: 13237 rev_number: 2 eprint_status: archive userid: 1 dir: disk0/00/01/32/37 datestamp: 2023-11-10 03:27:48 lastmod: 2023-11-10 03:27:48 status_changed: 2023-11-10 01:50:40 type: conference_item metadata_visibility: show creators_name: Puspitasari, P. creators_name: Permanasari, A.A. creators_name: Shaharun, M.S. creators_name: Muhammad, A. title: High saturation superparamagnetic properties of low-temperature sintering of nickel oxide ispublished: pub note: cited By 2; Conference of 2019 Annual International Conference on Renewable Energy, ICORE 2019 ; Conference Date: 9 August 2019 Through 10 August 2019; Conference Code:164592 abstract: Application of nickel oxide as magnetic nanofluid become more interesting. This research aims to synthesized nickel oxide as magnetic material and analyzed its behaviour under low sintering temperature. This research used synthesized nickel oxide with sol-gel method heated at two temperature variations. The first sample heated at 220º C until self-combustion process occurred; and the second sample heated at 80º C until it turned into a gel, similar to the general sol-gel process. After that, all samples received sintering treatment at 400º C. This research used XRD test resulted in peaks appearances in all samples, indicating all samples were single-phase samples. The first sample showed a crystallite structure size of 72.66 nm before sintering and 39.64 after sintering, whereas the second sample displayed a crystallite structure size of 48.46 nm before sintering and 62.28 nm after sintering. The SEM test result exhibited agglomerated particles and sphere morphology. The FTIR test results presented differences as-prepared sample of solgel method. The functional groups and bonds show broadening peak at O-H bond. Lastly, the VSM test results showed a soft magnetic material with superparamagnetic properties and has high saturation magnetic in the second sample. © 2020 American Institute of Physics Inc.. All rights reserved. date: 2020 publisher: American Institute of Physics Inc. official_url: https://www.scopus.com/inward/record.uri?eid=2-s2.0-85096435963&doi=10.1063%2f5.0000884&partnerID=40&md5=4ff7d32617ffa2bc71a20b544a653114 id_number: 10.1063/5.0000884 full_text_status: none publication: AIP Conference Proceedings volume: 2228 refereed: TRUE isbn: 9780735419872 issn: 0094243X citation: Puspitasari, P. and Permanasari, A.A. and Shaharun, M.S. and Muhammad, A. (2020) High saturation superparamagnetic properties of low-temperature sintering of nickel oxide. In: UNSPECIFIED.