eprintid: 12340 rev_number: 2 eprint_status: archive userid: 1 dir: disk0/00/01/23/40 datestamp: 2023-11-10 03:26:53 lastmod: 2023-11-10 03:26:53 status_changed: 2023-11-10 01:48:35 type: conference_item metadata_visibility: show creators_name: Lee, X.Y. creators_name: Chew, T.L. creators_name: Oh, P.C. creators_name: Ho, C.-D. creators_name: Ong, Y.T. title: Synthesis and characterization of MSU-2 for CO2 adsorption ispublished: pub note: cited By 1; Conference of 5th International Conference of Chemical Engineering and Industrial Biotechnology, ICCEIB 2020 ; Conference Date: 9 August 2020 Through 11 August 2020; Conference Code:166005 abstract: The advancement of adsorption technology is highly dependent on the characteristics of the adsorbents used. However, the commonly used one-dimensional (1D) MCM-41 and two-dimensional (2D) SBA-15 were found to induce gas diffusion difficulty. With this, MSU-2 was introduced as it shows high potentiality to be employed as CO2 adsorbent due to its excellent properties such as the highly interconnected three-dimensional (3D) wormhole-like framework structure as well as large specific surface area, total pore volume and pore size. The focus of the current study focuses on the synthesis of MSU-2 and the investigation on the CO2 adsorption capacity of the synthesized MSU-2 at various temperatures and pressures. The preparation of the MSU-2 was achieved by fluoride-assisted two-step process of solution precipitation method involving the addition of tetraethylorthosilicate (TEOS) to the acidified aqueous solution of nonionic surfactant, Triton X-100. The resultant MSU-2 was characterized by SEM, TEM, SAP analyser, XRD, FTIR spectrometer and TGA. The analyzed results showed that MSU-2 with desired features was successfully synthesized. The CO2 gas adsorption studies of the MSU-2 was demonstrated at different temperatures (25 °C and 85 °C) and different pressures (1 bar and 5 bar) to study the effect of temperatures and pressures on the CO2 adsorption capacity of the MSU-2. The highest CO2 adsorption capacity of the MSU-2 was found to be 0.98 mmol-CO2/gadsorbent when the operating conditions were set at 25 °C and 5 bar. This adsorption experiment also deduced that low adsorption temperature and high operating pressure promote adsorption process which give higher CO2 adsorption capacity. © 2020 Institute of Physics Publishing. All rights reserved. date: 2020 publisher: IOP Publishing Ltd official_url: https://www.scopus.com/inward/record.uri?eid=2-s2.0-85099143504&doi=10.1088%2f1757-899X%2f991%2f1%2f012076&partnerID=40&md5=a0e12e02dd55e3930ed6760893e08145 id_number: 10.1088/1757-899X/991/1/012076 full_text_status: none publication: IOP Conference Series: Materials Science and Engineering volume: 991 number: 1 refereed: TRUE issn: 17578981 citation: Lee, X.Y. and Chew, T.L. and Oh, P.C. and Ho, C.-D. and Ong, Y.T. (2020) Synthesis and characterization of MSU-2 for CO2 adsorption. In: UNSPECIFIED.