eprintid: 12231
rev_number: 2
eprint_status: archive
userid: 1
dir: disk0/00/01/22/31
datestamp: 2023-11-10 03:26:46
lastmod: 2023-11-10 03:26:46
status_changed: 2023-11-10 01:17:11
type: article
metadata_visibility: show
creators_name: Zaid, H.M.
creators_name: Fakhruldin, H.
creators_name: Yow, F.Y.
creators_name: Razali, N.
creators_name: Dasan, Y.K.
title: Synthesis and characterization of titanium dioxide nanoparticles for application in enhanced oil recovery
ispublished: pub
keywords: Calcination; Crystallite size; Enhanced recovery; Field emission microscopes; High resolution transmission electron microscopy; Nanocrystals; Nanoparticles; Oxides; Particle size; Scanning electron microscopy; Sol-gel process; Sol-gels; Synthesis (chemical); Titanium dioxide; X ray diffraction, Average particle size; Calcination temperature; Enhanced oil recovery; Field emission scanning electron microscopy; Nanocrystallines; Powder X ray diffraction; Reaction parameters; Synthesis and characterizations, TiO2 nanoparticles
note: cited By 2
abstract: In this study, titanium dioxide nanoparticles were synthesized for possible application in enhanced oil recovery. Sol-gel method was employed with titanium(IV) isopropoxide as the precursor. The prepared materials were characterized using Powder X-Ray Diffraction (XRD), Field Emission Scanning Electron Microscopy (FESEM), High-Resolution Transmission electron microscopy (HRTEM) and Brunauer�Emmet�Teller (BET) techniques. Reaction parameter such as calcination temperature was varied during the preparation to obtain the uniform TiO2 nanoparticles with the smallest particle size and high surface area. The results of study revealed that 400C is the optimum calcination temperature in preparing TiO2 nanoparticles producing the smallest crystallite and particle sizes. XRD results indicated that the nanoparticles have formed anatase phase at 400C and achieved low crystallite size of 7.27 nm with the smallest average particle size of 19.53 nm through FESEM and HRTEM observations. BET analysis had achieved the highest surface area 103.64 m2/g. © 2019 Trans Tech Publications, Switzerland
date: 2019
publisher: Trans Tech Publications Ltd
official_url: https://www.scopus.com/inward/record.uri?eid=2-s2.0-85062705139&doi=10.4028%2fwww.scientific.net%2fDDF.391.74&partnerID=40&md5=7179ad321e612e8f8905e247a8f2d634
id_number: 10.4028/www.scientific.net/DDF.391.74
full_text_status: none
publication: Defect and Diffusion Forum
volume: 391
pagerange: 74-81
refereed: TRUE
issn: 10120386
citation:   Zaid, H.M. and Fakhruldin, H. and Yow, F.Y. and Razali, N. and Dasan, Y.K.  (2019) Synthesis and characterization of titanium dioxide nanoparticles for application in enhanced oil recovery.  Defect and Diffusion Forum, 391.  pp. 74-81.  ISSN 10120386