Pressureless sintering and characterization of Al2O 3-SiO2-ZrO2 composite

Asmelash, G.M. and Mamat, O. (2012) Pressureless sintering and characterization of Al2O 3-SiO2-ZrO2 composite. Defect and Diffusion Forum, 329. pp. 113-128. ISSN 10120386

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Abstract

An oxide ceramic-based composite in the Al2O3-SiO 2-ZrO2 (ASZ) system was developed and investigated using a pressureless sintering route. The effect of the content of each component and sintering temperature upon the microstructure, density, hardness and strength was studied. X-ray diffraction (XRD) and field emission scanning electron microscopy (FESEM) were used to investigate the phase transformation sequences of the ASZ composite system. The flexural strength was measured using three-point bending method on a universal testing machine, while the Indentation Fracture (IF) method was used to determine the fracture toughness of the composite. The results showed that, with varying ZrO2 content, keeping the silica content constant and the alumina as a matrix, densification tends to decrease as the content of zirconia increases from 20 wt. of the composition. X-ray diffraction peaks indicated fully developed alumina, mullite and zirconia phases due to solid-phase reaction and liquid-phase sintering of the system. The experimental results also revealed that, for a sintering temperature of 1500°C, the hardness value ranged from 12 GPa to 14 GPa and the flexural strength was 420±31MPa.The fracture toughness (K Ic) was also reported to be between 4.5 and 5.1 MPa.m1/2, for samples sintered at a temperature of 1450°C. © (2012) Trans Tech Publications, Switzerland.

Item Type: Article
Additional Information: cited By 4
Uncontrolled Keywords: Alumina; Aluminum oxide; Bending strength; Field emission microscopes; Fracture testing; Fracture toughness; Hardness; Liquid phase sintering; Mullite; Scanning electron microscopy; Silica; Silicate minerals; X ray diffraction; Zirconia, Field emission scanning electron microscopy; Indentation fracture; Pressure-less sintering; Sintering temperatures; Solid phase reaction; Three point bending methods; Transformation sequences; Universal testing machines, Sintered alumina
Depositing User: Mr Ahmad Suhairi UTP
Date Deposited: 09 Nov 2023 15:51
Last Modified: 09 Nov 2023 15:51
URI: https://khub.utp.edu.my/scholars/id/eprint/2898

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