Microstructure, phase compositions and mechanical properties of slip cast sintered SiC/Si3N4 composites

Shahrestani, S. and Ismail, M.C. and Kakooei, S. and Beheshti, M. (2021) Microstructure, phase compositions and mechanical properties of slip cast sintered SiC/Si3N4 composites. Ceramics International, 47 (9). pp. 13173-13180. ISSN 02728842

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Abstract

In this study, a slurry containing a mixture of Si and SiC powders was used to fabricate the SiC/Si3N4 composites by slip casting method and sintering in a nitrogen-controlled furnace. The effects of mixing ratios of Si and SiC powders, different particle sizes of SiC powders as well as three sintering temperatures (1400, 1450, 1490 °C) were evaluated for SiC�Si3N4 composites. The results demonstrated that the best slurry was prepared using the weight ratio of Si/SiC of 30/70 and the fine-particle size of SiC powders with an average particle size of d50 � 0.45 μm. The results of XRD and FESEM determined that the sintered composites at 1450 °C have the minimum porosity without the SiO2 phase. Besides, with an increase in the sintering temperature, the α/β-Si3N4 phase ratio increased while the hardness and flexural strength were strongly dependent on the α/β-Si3N4 phase ratio in the SiC�Si3N4 composites. © 2021 Elsevier Ltd and Techna Group S.r.l.

Item Type: Article
Additional Information: cited By 4
Uncontrolled Keywords: Mechanical properties; Particle size; Powders; Silica; Silicon; Silicon carbide; Sintering, Average particle size; Different particle sizes; Fine particles; Mixing ratios; Sintered SiC; Sintering temperatures; Slip casting method; Weight ratios, Nitrogen compounds
Depositing User: Mr Ahmad Suhairi UTP
Date Deposited: 10 Nov 2023 03:29
Last Modified: 10 Nov 2023 03:29
URI: https://khub.utp.edu.my/scholars/id/eprint/14995

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